Amaç: Çalışmamızın amacı, son yıllarda kullanımı yaygınlaşan, bulk fill kompozit rezinlerin, farklı ışık cihazları ile polimerizasyonunun, su emilimi ve çözünürlük değerleri üzerine olan etkisini incelemektir. Gereç ve Yöntemler: Çalışmamızda 8 farklı bulk fill kompozit rezin; SDR (Dentsply), Sonicfill (Kerr), x-traFil (Voco), Beautifil Bulk Restorative (Shofu), Beautifil Bulk Flowable (Shofu), Filtek Bulk Fill Flowable (3M ESPE), Admira Fusion X-tra (Voco), Estelite Bulk Fill Flow (Tokuyama) ve mikrohibrit tipte Filtek Z250 Universal (3M ESPE) kullanılarak 6 mm çapında, 4 mm kalınlığında örnekler hazırlanmış, LED ve QTH ışık kaynakları ile polimerize edilmiştir. Örneklerin su emilim ve suda çözünürlük düzeylerini saptamak için, ISO 4049:2009 spesifikasyonu esas alınarak, standartta bildirilen formüllerden yararlanılmıştır. Kompozit ve ışığa göre çözünürlük ve su emilimi karşılaştırmalarında, Kruskal-Wallis, bağımsız örneklem t-testi ve Mann-Whitney U testleri uygulanmıştır. Farkın belirlenmesinde, ''post hoc'' Bonferroni testi kullanılmıştır. Önem düzeyi p<0,05 olarak alınmıştır. Bulgular: Işık cihazlarının hem su emilimi hem de çözünürlük üzerinde etkisi anlamlı bulunmuştur (p<0,05). Beautifil-Bulk Restorative kompozit grubunda çözünürlük değeri, Admira Fusion X-tra ve Estelite Bulk Fill Flow grupları ile karşılaştırıldığında anlamlı derecede yüksektir (p=0,001 ve p=0,041). En yüksek su emilimi ortalama değeri, Beautifil-Bulk Restorative ve QTH etkileşimi ile elde edilmiştir ve 20,37'dir. En düşük su emilimi ortalama değeri, x-traFil kompozitinde hem LED hem QTH ile 8,8'dir. Sonuç: Kompozit rezinlerin yapısı ve polimerizasyonda kullanılan ışık cihazları, su emilimi ve çözünürlük düzeylerini etkilemektedir.
Anahtar Kelimeler: Absorpsiyon; çözünürlük; ışık kaynağı; kompozit dental rezin
Objective: The aim of our study is to examine the effects of polymerization of bulk fill composite resins, which have become widely used in recent years, with different light devices on water absorption and solubility levels. Material and Methods: Samples with a diameter of 6 mm and a thickness of 4 mm were prepared by using 8 different bulk fill composite resins SDR (Dentsply), Sonicfill (Kerr),x-traFil (Voco), Beautifil Bulk Restorative (Shofu), Beautifil Bulk Flowable (Shofu), Filtek Bulk Fill Flowable (3M ESPE), Admira Fusion X-tra (Voco),Estelite Bulk Fill Flow (Tokuyama) and microhybrid Filtek Z250 Universal (3M ESPE) and they were polymerized with LED and QTH light sources.In order to determine the water absorption and water solubility levels of the samples,the formulas reported in the standard were used,based on ISO 4049:2009 specification. Kruskal-Wallis, Independent Sample T and Mann-Whitney U tests were applied for solubility and water absorption comparisons according to composite and light. ''Post hoc'' Bonferroni test was used to determine the difference. Significance level was taken as p<0.05. Results: The effect of light devices on both water absorption and solubility was significant (p<0.05). The solubility value was significantly higher in the Beautifil Bulk Restorative composite group compared to the Admira Fusion X-tra and Estelite Bulk Fill Flowable groups (p=0.001 and p=0.041).The highest mean value of water absorption was obtained with the interaction of Beautifil Bulk Restorative and QTH and was 20.37. The lowest mean value of water absorption was 8.8 in x-traFil composite with both LED and QTH. Conclusion: The structure of composite resins and light devices used in polymerization affect water absorption and solubility levels.
Keywords: Absorption; solubility; curing lights; composite dental resin
- Al Sunbul H, Silikas N, Watts DC. Resin-based composites show similar kinetic profiles for dimensional change and recovery with solvent storage. Dent Mater. 2015;31(10):e201-17. [Crossref] [PubMed]
- Tekin TH, Kantürk Figen A, Yılmaz Atalı P, Coşkuner Filiz B, Pişkin MB. Full in-vitro analyses of new-generation bulk fill dental composites cured by halogen light. Mater Sci Eng C Mater Biol Appl. 2017;77:436-45. [Crossref] [PubMed]
- Misilli T, Gönülol N. Water sorption and solubility of bulk-fill composites polymerized with a third generation LED LCU. Braz Oral Res. 2017;31:e80. [Crossref] [PubMed]
- Kim RJ, Son SA, Hwang JY, Lee IB, Seo DG. Comparison of photopolymerization temperature increases in internal and external positions of composite and tooth cavities in real time: Incremental fillings of microhybrid composite vs. bulk filling of bulk fill composite. J Dent. 2015;43(9):1093-8. [Crossref] [PubMed]
- Chesterman J, Jowett A, Gallacher A, Nixon P. Bulk-fill resin-based composite restorative materials: a review. Br Dent J. 2017;222(5):337-44. [Crossref] [PubMed]
- Osiewicz MA, Werner A, Roeters FJM, Kleverlaan CJ. Wear of bulk-fill resin composites. Dent Mater. 2022;38(3):549-53. [Crossref] [PubMed]
- Gönülol N, Şen Tunç E, Özer S, Yıldızlı K. Evaluation of water sorption-solubility and surface roughness of different bulk fill composite resins. Meandros Med Dent J. 2019;20(1):28-33. [Crossref]
- Söderholm KJ, Mukherjee R, Longmate J. Filler leachability of composites stored in distilled water or artificial saliva. J Dent Res. 1996;75(9):1692-9. [Crossref] [PubMed]
- Szczesio-Wlodarczyk A, Sokolowski J, Kleczewska J, Bociong K. Ageing of dental composites based on methacrylate resins-a critical review of the causes and method of assessment. Polymers (Basel). 2020;12(4):882. [Crossref] [PubMed] [PMC]
- Ortengren U, Wellendorf H, Karlsson S, Ruyter IE. Water sorption and solubility of dental composites and identification of monomers released in an aqueous environment. J Oral Rehabil. 2001;28(12):1106-15. [Crossref] [PubMed]
- Yiu CK, King NM, Pashley DH, Suh BI, Carvalho RM, Carrilho MR, et al. Effect of resin hydrophilicity and water storage on resin strength. Biomaterials. 2004;25(26):5789-96. [Crossref] [PubMed]
- Göhring TN, Besek MJ, Schmidlin PR. Attritional wear and abrasive surface alterations of composite resin materials in vitro. J Dent. 2002;30(2-3):119-27. [Crossref] [PubMed]
- Ito S, Hashimoto M, Wadgaonkar B, Svizero N, Carvalho RM, Yiu C, et al. Effects of resin hydrophilicity on water sorption and changes in modulus of elasticity. Biomaterials. 2005;26(33):6449-59. [Crossref] [PubMed]
- Ferracane JL. Hygroscopic and hydrolytic effects in dental polymer networks. Dent Mater. 2006;22(3):211-22. [Crossref] [PubMed]
- Alshali RZ, Salim NA, Satterthwaite JD, Silikas N. Long-term sorption and solubility of bulk-fill and conventional resin-composites in water and artificial saliva. J Dent. 2015;43(12):1511-8. [Crossref] [PubMed]
- Alrahlah A, Silikas N, Watts DC. Hygroscopic expansion kinetics of dental resin-composites. Dent Mater. 2014;30(2):143-8. [Crossref] [PubMed]
- Gajewski VE, Pfeifer CS, Fróes-Salgado NR, Boaro LC, Braga RR. Monomers used in resin composites: degree of conversion, mechanical properties and water sorption/solubility. Braz Dent J. 2012;23(5):508-14. [Crossref] [PubMed]
- Wei YJ, Silikas N, Zhang ZT, Watts DC. Diffusion and concurrent solubility of self-adhering and new resin-matrix composites during water sorption/desorption cycles. Dent Mater. 2011;27(2):197-205. [Crossref] [PubMed]
- Jeong TS, Kang HS, Kim SK, Kim S, Kim HI, Kwon YH. The effect of resin shades on microhardness, polymerization shrinkage, and color change of dental composite resins. Dent Mater J. 2009;28(4):438-45. [Crossref] [PubMed]
- Leprince JG, Hadis M, Shortall AC, Ferracane JL, Devaux J, Leloup G, et al. Photoinitiator type and applicability of exposure reciprocity law in filled and unfilled photoactive resins. Dent Mater. 2011;27(2):157-64. [Crossref] [PubMed]
- Price RB, Shortall AC, Palin WM. Contemporary issues in light curing. Oper Dent. 2014;39(1):4-14. [Crossref] [PubMed]
- Gonulol N, Ozer S, Tunc ES. Effect of a third-generation LED LCU on microhardness of tooth-colored restorative materials. Int J Paediatr Dent. 2016;26(5):376-82. [Crossref] [PubMed]
- Zhang Y, Xu J. Effect of immersion in various media on the sorption, solubility, elution of unreacted monomers, and flexural properties of two model dental composite compositions. J Mater Sci Mater Med. 2008;19(6):2477-83. [Crossref] [PubMed]
- Bayrak GD, Yaman-Dosdogru E, Selvi-Kuvvetli S. The Effect of two different light-curing units and curing times on bulk-fill restorative materials. Polymers (Basel). 2022;14(9):1885. [Crossref] [PubMed] [PMC]
- Mortier E, Gerdolle DA, Jacquot B, Panighi MM. Importance of water sorption and solubility studies for couple bonding agent--resin-based filling material. Oper Dent. 2004;29(6):669-76. [PubMed]
- Neto CCL, das Neves AM, Arantes DC, Sa TCM, Yamauti M, de Magalhães CS, et al. Evaluation of the clinical performance of GIOMERs and comparison with other conventional restorative materials in permanent teeth: a systematic review and meta-analysis. Evid Based Dent. 2022. [Crossref] [PubMed]
- Han L, Cv E, Li M, Niwano K, Ab N, Okamoto A, et al. Effect of fluoride mouth rinse on fluoride releasing and recharging from aesthetic dental materials. Dent Mater J. 2002;21(4):285-95. [Crossref] [PubMed]
- Gonulol N, Ozer S, Sen Tunc E. Water sorption, solubility, and color stability of giomer restoratives. J Esthet Restor Dent. 2015;27(5):300-6. [Crossref] [PubMed]
- McCabe JF, Rusby S. Water absorption, dimensional change and radial pressure in resin matrix dental restorative materials. Biomaterials. 2004;25(18):4001-7. [Crossref] [PubMed]
- Ilie N, Stark K. Curing behaviour of high-viscosity bulk-fill composites. J Dent. 2014;42(8):977-85. [Crossref] [PubMed]
- Bucuta S, Ilie N. Light transmittance and micro-mechanical properties of bulk fill vs. conventional resin based composites. Clin Oral Investig. 2014;18(8):1991-2000. [Crossref] [PubMed]
- Castro FL, Campos BB, Bruno KF, Reges RV. Temperature and curing time affect composite sorption and solubility. J Appl Oral Sci. 2013;21(2):157-62. [Crossref] [PubMed] [PMC]
- Sideridou I, Tserki V, Papanastasiou G. Study of water sorption, solubility and modulus of elasticity of light-cured dimethacrylate-based dental resins. Biomaterials. 2003;24(4):655-65. [Crossref] [PubMed]
- Sideridou ID, Achilias DS, Karabela MM. Sorption kinetics of ethanol/water solution by dimethacrylate-based dental resins and resin composites. J Biomed Mater Res B Appl Biomater. 2007;81(1):207-18. [Crossref] [PubMed]
.: Process List